Chemical Research in 1273-73-0

After consulting a lot of data, we found that this compound(1273-73-0)Application In Synthesis of Bromoferrocene can be used in many types of reactions. And in most cases, this compound has more advantages.

So far, in addition to halogen atoms, other non-metallic atoms can become part of the aromatic heterocycle, and the target ring system is still aromatic.Nesmeyanov, A. N.; Perevalova, E. G.; Lemenovskii, D. A.; Kosina, A. N.; Grandberg, K. I. researched the compound: Bromoferrocene( cas:1273-73-0 ).Application In Synthesis of Bromoferrocene.They published the article 《Ferrocenylgold-triphenylphosphine》 about this compound( cas:1273-73-0 ) in Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya. Keywords: gold ferrocenyl phosphines; ferrocenyl phosphines gold; phosphines gold ferrocenyl; ferrocenes; iron organic compound. We’ll tell you more about this compound (cas:1273-73-0).

To ferrocenyllithium from 2.8 g ferrocene in THF-Et2O with BuLi under argon was added 2 g ClAuPPh3, and after 2 hr the mixture quenched in H2O to yield 81% orange ferrocenyl-goldtriphenylphosphine, C5H5FeC5H4AuPPh3, decomposed 150°; ir and NMR spectral data given. Chromatog. on Al2O3 decomposed this to ferrocene. BrAuPPh3 in the above reaction gave the same complex in 67% yield. Treated with dry HCl in C6H6 the product gave ferrocene and ClAuPPh3, m. 242-3°; HI gave diferrocenyl in trace amounts along with nearly 100% ferrocene and IAuPPh3, m. 224-5°. HCN similarly converted the complex into ferrocene and AuCN.PPh3, m. 203.5-204°. Bromination gave bromoferrocene, m. 30-1°, and 81% BrAuPPh3. ClAuPPh3 in Et2O under argon treated with BuLi 5 hr gave 86% oily BuAuPPh3, which darkened in air. It was purified by freezing in liquid pentane at -70°.

After consulting a lot of data, we found that this compound(1273-73-0)Application In Synthesis of Bromoferrocene can be used in many types of reactions. And in most cases, this compound has more advantages.

Reference:
Thiazolidine – Wikipedia,
Thiazolidine – ScienceDirect.com