Category: 26364-65-8

New Advances in Chemical Research, May 2021. category: thiazolidine, Redox catalysis has been broadly utilized in electrochemical synthesis due to its kinetic advantages over direct electrolysis. 26364-65-8, Name is 2-Cyanoimino-1,3-thiazolidine, molecular formula is C4H5N3S. In a Article，once mentioned of 26364-65-8

A series of N-cyanoazomethines 1-12 has been synthesized, and their electronic properties studied by He(I) photoelectron (PE) spectroscopy using the composite molecule approach.This allows partial assignment of the ionization energies in the PE spectrum of cimetidine 16, a known H2-receptor antagonist.Determination of differential UV spectra of the model compounds 7 and 13 revealed that no intramolecular charge transfer (CT) interaction exists between the two “ends” of the cimetidine molecule, i.e. between the ?-electron rich imidazole ring and the relatively ?-electron deficient cyanoguanidine moiety.

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Abstract: Reaction of thiazolidin-2-cyanamide and substituted benzyl bromide compounds in acetonitrile at room temperature afforded the 3-(2?-substituted benzyl)thiazolidin-2-cyanamide derivatives 1?13 in good yields. Compounds 1?13 were characterized by proton nuclear magnetic resonance (1H NMR) and infrared spectroscopies, of which the structures of the isomeric o-, m-, and p-fluoro derivatives 4?6 were established by single crystal X-ray crystallography. Compound 4 crystallizes in the monoclinic space group P21/n, with a = 9.177(19), b = 8.551(18), c = 14.090(3) A, beta = 98.243(3), and Z = 4. The unit cell of 5 has a monoclinic P21/c symmetry with the cell parameters a = 9.289(2), b = 14.057(4), c = 8.574(2) A, beta = 100.350(3), and Z = 4. The unit cell of 6 also has a monoclinic P21/c symmetry with the cell parameters a = 9.333(4), b = 14.034(5), c = 8.508(3) A, beta = 99.15(5), and Z = 4. Graphic Abstract: A series of 3-(2?-substituted benzyl)thiazolidin-2-cyanamide derivatives were efficiently synthesized via the reaction of benzyl bromide compounds with thiazolidin-2-cyanamide, of which the structures of the isomeric o-, m-, and p-fluoro derivatives were characterized by X-ray crystallography. [Figure not available: see fulltext.]

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The reaction of 3-substituted 2-(N-cyanoimino)thiazolidine (NCT) derivatives with hydrazine hydrate afforded two types of 1,2,4-triazoles via a selective C2-S or C2-N3 bond fission, in which the selectivity was controlled by the N3-substituent.

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Reference of 26364-65-8, A catalyst don’t appear in the overall stoichiometry of the reaction it catalyzes, but it must appear in at least one of the elementary reactions in the mechanism for the catalyzed reaction. 26364-65-8, Name is 2-Cyanoimino-1,3-thiazolidine, molecular formula is C4H5N3S. In a Patent，once mentioned of 26364-65-8

A thiacloprid phase synthetic method (by machine translation)

The present invention provides a kind of thiacloprid phase synthetic method, comprises the following steps: adding to a reaction vessel 2 – chloro – 5 – chloromethyl pyridine and 2 – cyano imino – 1, 3 – thiazolidine, and water used as solvent, stirring the reaction, after-treatment, to get the object product thiacloprid. Wherein post-processing comprises: stirring cooling, filtering the reaction solution, adopting filter cake, to get the thiacloprid product; in the filtrate water and catalyst can be applied to a number of reaction in the next, and water and catalyst application times can be up to 10 or more times. The present invention provides aqueous phase synthesis method of thiacloprid of easy availability of raw materials, the process flow is short, mild operating conditions, almost no discharge of waste water, process and environmental protection; the Imidacloprid states sai phase synthetic method not only can obtain higher product yield and higher the purity of the product, but also can exhibit the process environment friendly, simple operation steps characteristic, therefore very suitable for large-scale industrial production. (by machine translation)

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Related Products of 26364-65-8, One of the major reasons for studying chemical kinetics is to use measurements of the macroscopic properties of a system, such as the rate of change in the concentration of reactants or products with time.In a article, authors is , mentioned the application of Related Products of 26364-65-8, Name is 2-Cyanoimino-1,3-thiazolidine, molecular formula is C4H5N3S

A including fluorine cyanogen imine thiazolidine substituted wicked two zuozuo kinds insecticide (by machine translation)

The present invention provides a including fluorine cyanogen imine thiazolidine substituted wicked two zuozuo kinds insecticide, the structure shown in formula I: The formula I compound Diamondback moth, Spodoptera exigua insecticidal, rice and the galenical, hot pepper anthrax bacteria, rice sheath blight fungus, Chinese rose inhibition of downy mildew and the like, can be used as agricultural or forestry plant pest control of the saw. (by machine translation)

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Related Products of 26364-65-8, Catalysts function by providing an alternate reaction mechanism that has a lower activation energy than would be found in the absence of the catalyst. In some cases, the catalyzed mechanism may include additional steps.In a article, 26364-65-8, molcular formula is C4H5N3S, introducing its new discovery.

3 – (2, 6 – Difluorophenyl) – 1, 2, 4 – oxdiazole compound and use thereof (by machine translation)

The present invention provides a 3 – (2, 6 – difluorophenyl) – 1, 2, 4 – oxdiazole compound miticides, the structure as shown in formula I: In the formula R is selected from: The formula I compound has excellent insecticidal or acaricidal activity, can be used for agriculture or forestry common pest control of mites. (by machine translation)

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Quinuclidine – Wikipedia,
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In homogeneous catalysis, the catalyst is in the same phase as the reactant. The number of collisions between reactants and catalyst is at a maximum.In a patent, 26364-65-8, name is 2-Cyanoimino-1,3-thiazolidine, introducing its new discovery. COA of Formula: C4H5N3S

A Convenient and General Method for the Preparation of tert-Butoxycarbonylaminoalkanenitriles and Their Conversion to Mono-tert-butoxycarbonylalkanediamines

A new method is described for the synthesis of tert-butoxycarbonylaminoalkanenitriles 3 by dehydration of the corresponding carboxamides 2 (prepared in two steps from aminoalkanoic acids) in the presence of trifluoroacetic anhydride and triethylamine.N-Boc-aminoalkanenitriles 3 are easily converted to mono-N-Boc-alkanediamines 4 under mild conditions avoiding the cleavage of the N-protective group.The monoprotected alkanediamines 4 are useful tools in affinity chromatography.

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Anomalous One-pot Transformation of 3-Dimethoxymethyl-2-(N-cyanoimino)thiazolidine into 6-Unsubstituted 2,4-Diamino-s-triazines by the Reaction with Amines

3-Dimethoxymethyl-2-(N-cyanoimino)thiazolidine 1e reacts with secondary amines to afford 2,4-diamino-s-triazines 4 unexpectedly, while the triazine 5 bearing different amino groups at 2 and 4 positions is selectively obtained by the reaction with a mixture of two kinds of amines.

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A new sulfenylation reagent, 3-phenylsulfenyl-2-(N- cyanoimino)thiazolidine, and its optically active version

We have developed a new sulfenylation reagent, 3-phenylsulfenyl-2-(N- cyanoimino)thiazolidine 3, that is readily available and stable upon storage. Compound 3 easily reacts with amines or thiols to give the corresponding sulfenamides or asymmetrical disulfides in excellent yields. It was also found that the alpha-sulfenylation reaction of carbonyl compounds with 3 proceeds smoothly. Furthermore, optically active 4-diphenylmethyl derivative 4 was synthesized as an asymmetric sulfenylation reagent, which realized 96% e.e. upon alpha-sulfenylation of a cyclic beta-keto ester.

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Quinuclidine – Wikipedia,
Quinuclidine | C7H633N | ChemSpider

In heterogeneous catalysis, the catalyst is in a different phase from the reactants. Product Details of 26364-65-8, At least one of the reactants interacts with the solid surface in a physical process called adsorption in such a way. 26364-65-8, name is 2-Cyanoimino-1,3-thiazolidine. In an article，Which mentioned a new discovery about 26364-65-8

PROCEDURE FOR THE PREPARATION OF 2-CYANOIMINO-1,3-THIAZOLIDINE

The disclosure provides for methods for preparing 2-cyanoimino-l,3-thiazolidine, which is an important building block for the preparation of crop protection active ingredients and pharmaceuticals. To this end, the disclosure provides for more efficient and improved methods of preparing 2-cyanoimino-l,3-thiazolidine.

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Quinuclidine – Wikipedia,
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