Research on new synthetic routes about 2199-44-2

I hope my short article helps more people learn about this compound(Ethyl 3,5-Dimethyl-2-pyrrolecarboxylate)Quality Control of Ethyl 3,5-Dimethyl-2-pyrrolecarboxylate. Apart from the compound(2199-44-2), you can read my other articles to know other related compounds.

In organic chemistry, atoms other than carbon and hydrogen are generally referred to as heteroatoms. The most common heteroatoms are nitrogen, oxygen and sulfur. Now I present to you an article called Improved synthesis of covalently strapped porphyrins. Application to highly deformed porphyrin synthesis, published in 1988-04-01, which mentions a compound: 2199-44-2, mainly applied to porphyrin strapped; polymethyleneporphyrin, Quality Control of Ethyl 3,5-Dimethyl-2-pyrrolecarboxylate.

The title porphyrins I (n = 1, 2, 3) were prepared α,ω-Dicarboxyalkyl dichloride, was treated with 2 equiv of 2-(ethoxycarbonyl)-3,5-dimethylpyrrole, and the chain-linked bis[5-(ethoxycarbonyl)pyrrole] so obtained was transformed into the pyrrole-2-carboxaldehyde by using standard methodol. Protection of the formyl groups as the dicyanovinyl derivative and the activation of the 2-Me substituents with SO2Cl2 gave the bis[2-(chloromethyl)pyrrol)], which on reaction with a 5-unsubstituted 2-pyrrolecarboxylate, in warm AcOH, afforded the chain-linked dipyrromethane dimer in high yield. Regeneration of the formyl substituents and removal of the ester group produced the 5-formyldipyrromethane dimer II, which was cyclized intramolecularly, under high dilution, to give I. II (n = 0) failed to cyclize.

I hope my short article helps more people learn about this compound(Ethyl 3,5-Dimethyl-2-pyrrolecarboxylate)Quality Control of Ethyl 3,5-Dimethyl-2-pyrrolecarboxylate. Apart from the compound(2199-44-2), you can read my other articles to know other related compounds.

Reference:
Thiazolidine – Wikipedia,
Thiazolidine – ScienceDirect.com