26364-65-8, 2-Cyanoimino-1,3-thiazolidine is a thiazolidine compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: Thiazolidin-2-ylidene-cyanamide (0.317 g, 2.50 mmol) inacetonitrile (20 mL) was dropwise added to a stirred solutionof substituted benzyl bromide (2.5 mmol) and 14 mL NaOHaqueous solution (1 M). The mixture is stirred at room temperaturefor 8-10 h. The soild was collected by filtration,washed with n-hexane and dried in vacuo. 3-(2-methylbenzyl)thiazolidin-2-ylidene-cyanamide (1)white solid, yield: 0.494 g (85.4%), m.p.: 115-16 C. 1HNMR (400 MHz, CDCl3):delta (ppm) 2.34 (s, 3H, CH3),3.32 (t,J = 7.6 Hz, 2H, NCH2),3.74 (t, 2H, J = 7.6 Hz, SCH2),4.57(s, 2H, CH2),7.14-7.19 (m, 2H, Ph). IR (KBr disc, cm-1):2918, w, nu(CH); 2182, s, 2160 sh, v(C?N); 1573, s, v(C=N).
26364-65-8 2-Cyanoimino-1,3-thiazolidine 3700797, athiazolidine compound, is more and more widely used in various.
Reference£º
Article; Jia, Ai-Quan; Ma, Sen; Wang, Jun-Ling; Zhang, Qian-Feng; Journal of Chemical Crystallography; (2020);,
Thiazolidine – Wikipedia
Thiazolidine – ScienceDirect.com